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The adsorption of various molecules on a silver electrode is accompanied by an enormous increase in the intensity of the Raman scattered radiation by up to 106-fold compared to the intensity in the homogeneous phase The surface enhancement effect led to great interest during the 1970s among theoreticians and experimentalists, including non-electrochemists In spite of considerable effort, no satisfactory theoretical basis for this effect has yet been found The amplification factor depends on the wavelength of the exciting radiation and also very strongly on the electrode material In addition to the silver electrode, which is mostly used, copper (an increase of about 105) and gold (about 104) electrodes are also suitable for these studies In addition, some silver alloys or other materials can also be used, whose surface has been modified by a small amount of silver.

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0 1.0

Increases in the Raman scattering radiation have also been reported for Ni, Pd, Cd, Hg, Pt and Al electrodes Methods employing X-rays and y-radiation are used less often in electrochemistry The possibility of using X-ray diffraction for in situ study of the electrode surface was first demonstrated in 1980 This technique has long been used widely as a method for the structural analysis of crystalline substances Diffraction patterns that are characteristic for the electrochemical interface can be obtained by using special electrochemical cells and elec-.

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open pdf file in a new window - CodeGuru Forums
12 Jul 2006 ... how can a pdf file be opened in a new window ? ... Thread: open pdf file in a new window .... FYI: I'm using asp . net with vb.net code behind .

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With CPU bandwidths and memory sizes increasing, attention also must be paid to data paths. For example, AMD plans to double data-path bandwidth over the next few years. In addition, blades and virtualization are creating a shared disk environment that was never designed to be shared. This will force a change in the way both operating systems and the hypervisors handle disk I/O (for example, a change in protocols and drivers to allow disk to be shared nicely), as well as the way storage vendors build their disk subsystems. Enhancements in virtualized I/O will continue to improve the way blade systems share common components. Watch for changes in PCI Express as well. There is no doubt that the combination of blades and virtualization technologies will stress all the system components as well as the management capabilities. In the past when this has happened, technological breakthroughs have been found. It will be exciting to watch as server virtualization consolidates workloads and increases utilization, while processors, memory, and I/O race to keep up.

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Figure 11.15. Changes in both diffraction ef ciency and modulation of refractive index as a function of draw ratio, for the grating remained in the lm 7 months after the recording (Fig. 11.14). Source: Zhao et al., 2003. Reprinted with permission.

trodes The electrode can also be studied in situ by measuring absorption of X-ray radiation The extended X-ray absorption fine structure (EXAFS) method is based on the excitation of core-level electrons and, in addition to elemental analysis, permits study of the electronic structure of surfaces The EXAFS method requires a quite intense source of X-ray radiation, preferably a synchrotron Mossbauer spectroscopy can be used for in situ study of electrodes containing nuclei capable of resonance absorption of y radiation; for practical systems, primarily the 57Fe isotope is used (passivation layers on iron electrodes, adsorbed iron complexes, etc) It yields valuable information on the electron density on the iron atom, on the composition and symmetry of the coordination sphere around the iron atom and on its oxidation state Methods employing electron and ion beams.

Power and cooling will continue to drive changes at the chip level as well as at the blade and chassis level, creating more efficiency in both power and cooling. In terms of mass movement, although liquid provides a far better cooling medium than air (think of the differences between an old VW bug and a Porsche) the economics of liquid cooling will continue to be a deterrent to many. Liquid cooling at the chip level may appear in niche products.

Of the methods employing a beam of electrons or ions for excitation of the sample and/or detection of the signal, various surface analysis methods are of greatest importance Qualitative and semiquantitative elemental analysis of the electrode surface is more or less routine for practically all the elements in the periodic system Nonetheless, the individual methods vary, among other factors, in their sensitivity for various elements, information depth (ie the thickness of the sample layer yielding a detectable signal) and lateral resolution The latter is determined by the surface area of the sample irradiated by the excitation beam With a beam of charged species, sufficiently intense radiation can be obtained even for focusing to very small cross-sections, which is the principle of microanalysis (microprobes) Scanning of the surface of the sample by the excitation beam yields the distribution of the elements over the sample surface (scanning microanalysis).

Transmittance (a.u.)

The basic methods of surface analysis are listed in Table 54 The X-ray photoelectron spectroscopic (XPS) method, also termed electron spectroscopy for chemical analysis (ESCA), one of the most frequently used methods, is based on the determination of the kinetic energy of the electrons emitted from the core levels in a photoelectric process The energy of the core levels is assessed with the help of the kinetic energy of the photoelectrons These energies unambiguously characterize the given atom The measurement is quite precise (with an error of about 10"1 eV) and thus not only can elemental analysis be carried out but also fine changes in the core level energies produced by changes in the electron densities due to the formation of chemical bonds, ie chemical shifts, can be studied.

9.0 Transmittance (a.u.)