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Like P(tBA-co-AA)-b-PAzoMA, most amphiphilic BCPs are not soluble in water, in contrast to small-molecule surfactants As aforementioned, to prepare their micelles or vesicles, the BCP needs to be dissolved rst in an organic solvent that is good for both blocks and then by adding water into the solution The aggregation of the hydrophobic blocks can occur at a critical water content, leading to the formation of the micellar aggregates A convenient way to investigate the effect of solvent on the photoinduced processes is to measure and compare the change in transmittance of the BCP solution as a function of added water content in the absence of and under UV irradiation Using a same solvent, such experiment can also be carried out to reveal the effect of the BCP composition by comparing the behaviors of two BCP samples subjected to the same experimental conditions Fig 6.

The bremsstrahlung background can be considerably suppressed by excitation of X-ray spectra using an ion beam {proton-induced X-ray emission, PIXE, or helion-induced X-ray emission, HIXE) The impact of an ion beam on the electrode surface can result in the transfer of the kinetic energy of the ions to the surface atoms and their release into the vacuum as a wide range of species atoms, molecules, ions, atomic aggregates (clusters), and molecular fragments This is the effect of ion sputtering The SIMS {secondary ion mass spectrometry) method deals with the mass spectrometry of sputtered ions The SIMS method has high analytical sensitivity and, in contrast to other methods of surface analysis, permits a study of isotopes In materials science, the SIMS method is the third most often used method of surface analysis (after AES and XPS); it has so far been used only rarely in electrochemistry.

Methods based on the study of the scattering of an ion beam also belong among techniques for analysis of surfaces that have been used only occasionally in electrochemistry The ion-scattering spectroscopic (ISS) method studies the scattering of slow ions (with energy up to 1 keV) The.

8 shows an example of the results Figures 68a and b compare P(tBA46-co-AA22)-b-PAzoMA74 dissolved in dioxane and tetrahydrofuran (2 mL, 1 mg mL 1), respectively, prior to the addition of water (% in volume with respect to the volume of the organic solvent) With and without UV irradiation (18 mW cm 2), the polymer solution following each addition of water was stirred for 3 min before the transmittance was measured In the case of the dioxane solution, without UV irradiation, the transmittance starts to decrease signi cantly after addition of about 13% of water, which corresponds to the formation of polymer vesicles Under UV light, the polymer aggregation process begins at a much higher water content of about 21%, and the transmittance drops more quickly than the solution without UV irradiation.

In-band management is the traditional method of management, in which management access and processing is done by the host system. This means that management requests, functions, and responses are carried out by the operating system and over the data network on which the target system is located. This has the advantages that no additional hardware, network, or processing environment is required. One big disadvantage is that if the network or targeted platform is not operational, then no remote management will be available either. The other disadvantage is that if the intent is to measure performance or resource utilization, using in-band techniques will impact the results as the processing and network activity associated with the test will impact the measurement. It is also possible that in-band management could have a negative impact on the system itself, using resources that may already be over utilized.

339 scattering of fast ions (with energy of about 1 MeV) has been studied by the Rutherford backscattering spectroscopic (RBS) method The scattering of ions from a surface can be described over the whole energy range as an elastic binary collision Determination of the energy and angle of the scattered ions yields, in the first place, information on the mass of the surface atoms, ie elemental analysis The RBS method is especially useful for the detection of heavy atoms at an electrode made of a light element It is employed for non-destructive analysis of depth concentration profiles In addition to the above methods, yielding primarily semiquantitative elemental analysis of the surface, further methods of electron and ion optics are suitable for the study of electrochemical systems The diffraction of slow electrons (low energy electron diffraction, LEED) is widely employed for structural investigation of single-crystal electrodes.

This result shows that in the mixed solvent of dioxane water, the increase in polarity of the PAzoMA block accompanying the conversion of transazobenzene onto cis-azobenzene has shifted the hydrophilic hydrophobic balance in such a way that the critical water content for the aggregation of PAzoMA block forming the vesicle is increased from 13% to 21% And the magnitude of the change determines the window in which the photoinduced dissociation and reformation of the vesicles can be observed In other words, only the vesicles formed at water content between about 15% and 20% could display a clear lightcontrolled dissociation and reformation Vesicles formed at higher water content cannot be disrupted by UV light because of the aggregation of this BCP under UV irradiation (with azobenzene moieties in the cis form).