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When the writing UV laser is turned on, the photoisomerization in the excited (reactive) regions converts oriented trans-azobenzene into disordered cis-azobenzene,.

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Fig. 5.36 Scheme of a scanning tunnelling microscope deposited atoms or molecules on metal and semiconductor electrodes, effects of surface reconstruction and electrochemical roughening, etc. The latter was demonstrated, for example after successive oxidation and reduction of the electrode surface in aqueous electrolytes, which is widely used for 'activation' of Au or Pt electrodes. Fundamental ESTM studies are performed prevailingly with single-crystal electrodes. The ESTM experiment provides actually five measurable quantities: tunnelling current, / at the applied voltage, Uy and three dimensions, x, y, z. The standard STM can therefore easily be modified by recording the local l-Uy U-Zy.ox I-z characteristics (z is vertical distance of the tip from the electrode surface). Plot of dl/dU or d//dz versus x and y brings additional information on the electronic and chemical surface properties (local work functions, density-of-states effects, etc.), since these manifest themselves primarily as I-U dependences. The mentioned plots are basis of the scanning tunnelling spectroscopy (STS). Other techniques derived from tunnelling microscopy are based on the measurement of small repulsive forces (down to 10~9N) acting on a diamond tip attached on the gold foil. These forces originate from repulsion of individual atoms between the tip and the examined surface {atomic force microscope, AFM). Unlike standard tunnelling microscopy, the AFM is not confined only to electrically conducting samples. Other methods based on the concept of a force microscopy are laser force microscope (LFN) which works with attractive rather than repulsive forces, and magnetic force

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corresponding to an isothermal photochemical phase transition from the LC to the isotropic phase As the azobenzene polymer in the isotropic phase is more uid than that in the LC state, its microdomains become less effective cross-linking points, which results in relaxation of oriented PB chains and release of the stress As this happens, the stress is no longer uniformly distributed in space as before irradiation, and local structural reorganization may follow to rebalance the stress along the SD This perturbation might be enough to disorder trans-azobenzene groups in nonexcited areas, which explains the erasure of the rst grating As the irradiation continues, the excited areas may undergo further structural changes because of the photoinduced isotropic state of the azobenzene polymer.

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microscope (MFM) The use of these methods in electrochemistry is so far only marginal Electrochemical background has, however, a recently developed scanning ion conductance microscope (SICM) In this case, the sample is immersed in an electrolyte bath and scanned by a fine electrolytefilled micropipette while measuring the ion current between two silver electrodes placed in the bath and inside the micropipette The obtained resolution (ca 10 nm) makes possible to monitor, for example, ion currents flowing through individual channels in biological membranes Radioactive tracer techniques In electrochemistry, the procedure is essentially the same as in studies of chemical reactions: the electroactive substance or medium (solvent, electrolyte) is labelled, the product of the electrode reaction is isolated and its activity is determined, indicating which part of the electroactive substance was incorporated into a given product or which other component of the electrolysed system participated in product formation.

A more elaborate and capable approach taken by newer blade server systems is the use of a management service processor, also called a management module. A management module is a complete (shared) management system with its own separate management processor, its own memory, and its own NIC. The service processor in the management module communicates with service processors on each blade via its own internal bus. The management module can perform all of the functions listed previously under BMCs, as well as providing other capabilities and protocols such as IPMI (see the next section) and KVM switching (these functions vary by vendor and product). The management module stores all event and error information and is the focal point for any troubleshooting, monitoring or active management of components within the chassis. It is known externally by its IP address and is accessible via a web browser.

Measurement of the exchange current at an amalgam electrode by means of a labelled metal in the amalgam (see page 262) is based on a similar principle These techniques are especially useful for studies of the adsorption of reactants, intermediates and products of electrode reactions The simplest case corresponds to adsorption that is so strong that the electrode can be removed from the solution, rinsed and its activity measured without interference from desorption When this procedure is impossible, the activity of the adsorbate can be measured by the 'electrode lowering method' The radioactive counter is placed under the bottom of the cell, which is made of a plastic foil The electrode can be located at large distances from the bottom or can be placed so close to the bottom that only a thin layer of solution remains beneath it.

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